Synthesis of Compounds C-2,8,14,20-TETRA- (2,4,5-Trimetoxy) Phenilic Calciums [4] Resorsinarents from 2,4,4-Trimetoxic Benzaldehyde Compounds

  • Yoktan E Buraen
  • Pius D Ola
  • Reinner I Lerrick
Keywords: Genoak (Acorus calamus), Asaron, 2,4,5-trimethoxy benzaldehyde, C-2,8,14,20-tetra-(2,4,5-trimethoxy)phenyl calix[4]recorcinarene

Abstract

The synthesis of C-2,8,14,20-tetra-(2,4,5-trimethoxy)phenyl calix[4] resorcinarene from 2,4,5-trimethoxy  benzaldehyde has been done. Through isolation of asaron from Timor Genoak (Acorus calamus) followed by its oxidation with K2Cr2O7, the C-2,8,14,20-tetra-(2,4,5-trimethoxy)phenyl calix[4] resorcinarene has, therefore, been accessed over reflux. The asaron has been isolated as 3.05% of yellow oil whilst, the oxidation produced 2,4,5-trimethoxy benzaldehyde with the yield of 49.49%. The C-2,8,14,20-tetra-(2,4,5-trimethoxy) phenyl calix[4]resorcinarene has been yielded as 89.29% of a brown solid.

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Published
2019-12-17
How to Cite
Buraen, Y., Ola, P., & Lerrick, R. (2019). Synthesis of Compounds C-2,8,14,20-TETRA- (2,4,5-Trimetoxy) Phenilic Calciums [4] Resorsinarents from 2,4,4-Trimetoxic Benzaldehyde Compounds. Jurnal Saintek Lahan Kering, 2(2), 46-48. https://doi.org/https://doi.org/10.32938/slk.v2i2.867
Section
Original research article